Synthesis and Characterization of Some New Benzodiazepinium Salt Derivatives under microwave Irradiation Abdel- Amir M. Fenjan | Ala'a Sh. Shubram

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Baghdad Science Journal

Abstract

An attempt to synthesize the benzoimidazol derivatives from the reaction of o-phenylenediamine and benzoic acid derivatives in the presence of ethanol and various ketones under microwave irradiation, 1 , 5 - benzodiazepinum salt derivatives were obtained instead of them. Unexpected reaction was happened for synthesis a new series of benzodiazepinium salt derivatives in a selective yield . The reaction mechanism was also discussed. The new compounds were purified and identified their structures were elucidated using various physical techniques like; FT- IR spectra, micro elemental analysis (C.H.N) and 1H NMR spectra.

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Journal BS. Synthesis and Characterization of Some New Benzodiazepinium Salt Derivatives under microwave Irradiation. BSJ [Internet]. 6Dec.2015 [cited 31May2020];12(4):753-60. Available from: http://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/2123
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