Synthesis and Characterization of Some New Monemer and Polymers Containing Hetero Cyclic Rings With Study of Their Physical Properties.

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Ibtisam K. Jassim
Iman M. M. Hassan

Abstract

Number of new polyester and polyamide are prepared as derivatives from 5,5`-(1,4-phenylene)-bis-(1,3,4-thiadiazole-2-amine) [C1], three series of heterocyclic compounds were synthesized.The first series includes the Schiff base [C2] prepared from the reaction between compound [C1] with p-hydroxy benzaldehyde in presence of acetic acid and absolute ethanol , then these derivatives have reaction with maleic anhydride , phthalic anhydride and sodium azide, respectively to obtain the compounds [C3-5] contaning (oxazepine and tetrazole) rings.The third series of compounds [C1-5] has transformed to their polymers [C6-15] by reaction with adipoyl chloride and glutroyl chloride , respectively. The reaction was followed by T.L.C and identified by FT-IR , 1H-NMR ,C.H.N analysis , softening point , viscosity, TGA , DSC and X-ray.

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Synthesis and Characterization of Some New Monemer and Polymers Containing Hetero Cyclic Rings With Study of Their Physical Properties. Baghdad Sci.J [Internet]. 2016 Jun. 5 [cited 2024 Mar. 28];13(2.2NCC):0172. Available from: https://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/2763
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How to Cite

1.
Synthesis and Characterization of Some New Monemer and Polymers Containing Hetero Cyclic Rings With Study of Their Physical Properties. Baghdad Sci.J [Internet]. 2016 Jun. 5 [cited 2024 Mar. 28];13(2.2NCC):0172. Available from: https://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/2763

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