Abstract
An attempt to synthesize the benzoimidazol derivatives from the reaction of o-phenylenediamine and benzoic acid derivatives in the presence of ethanol and various ketones under microwave irradiation, 1 , 5 - benzodiazepinum salt derivatives were obtained instead of them. Unexpected reaction was happened for synthesis a new series of benzodiazepinium salt derivatives in a selective yield . The reaction mechanism was also discussed. The new compounds were purified and identified their structures were elucidated using various physical techniques like; FT- IR spectra, micro elemental analysis (C.H.N) and 1H NMR spectra.
Keywords
Benzodiazepinium Salt, Microwave Irradiation, Characterization.
Article Type
Article
How to Cite this Article
Fenjan, Abdel- Amir M. and Shubram, Ala'a Sh.
(2015)
"Synthesis and Characterization of Some New Benzodiazepinium Salt Derivatives under microwave Irradiation,"
Baghdad Science Journal: Vol. 12:
Iss.
4, Article 14.
DOI: https://doi.org/10.21123/bsj.2015.12.4.753-760
