Synthesis and Characterization of New Polyimide by Curing Poly Acryloyl Chloride with Different Amides Entesar O. Al-Temimi|Mahmoud A.AL-Issa|Sameaa J. Al-Bayati

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Baghdad Science Journal

Abstract

The present work involved preparation of new substituted and unsubstituted and poly imides (1-17) using reaction of acryloyl chloride with different amides (aliphatic ,aromatic) in the presence of a suitable solvent and amount tri ethyl amine (Et3N) with heating – the structure confirmation of all polymers were proved using FT-IR,1H-NMR,C13NMR and UV spectroscopy ,thermal analysis (TG) for some polymers confirmed their thermal stabilities . Other physical properties including softening and melting points, PH and solubility of the polymers were also measured

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Journal BS. Synthesis and Characterization of New Polyimide by Curing Poly Acryloyl Chloride with Different Amides: Entesar O. Al-Temimi|Mahmoud A.AL-Issa|Sameaa J. Al-Bayati. Baghdad Sci.J [Internet]. 2013Sep.1 [cited 2021Aug.2];10(3):686-98. Available from: https://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/2582
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