Detection of Methamphetamine using Nanobentonite as a Novel Solid Phase Extraction Column Matrix Assisted with Gas Chromatography- Mass Spectroscopy

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Nur Asyiah Dalimunthe
https://orcid.org/0000-0002-0718-9390
Zul Alfian
http://orcid.org/0000-0001-9470-3505
Basuki Wirjosentono
https://orcid.org/0000-0002-7501-4947
Eddiyanto
https://orcid.org/0000-0001-6627-7705

Abstract

          This study was done to evaluate a new technique to determine the presence of methamphetamine in the hair using nano bentonite-based adsorbent as the filler of extraction column. The state of the art of this study was based on the presence of silica in the nano bentonite that was assumed can interact with methamphetamine. The hair used was treated using methanol to extract the presence of methamphetamine, then it was continued by sonicating the hair sample. Qualitative analysis using Marquish reagent was performed to confirm the presence of methamphetamine in the isolate.The hair sample that has been taken in a different period confirmed that this current developing method can be used to analyzed methamphetamine. This method has an average recovery percentage by 104%. This result was also supported by the precision, linearity, LOD and LOQ, i.e. 0.0775; 0.968; 0.00000256 and 0.000000775, respectively.

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1.
Dalimunthe NA, Alfian Z, Wirjosentono B, Eddiyanto. Detection of Methamphetamine using Nanobentonite as a Novel Solid Phase Extraction Column Matrix Assisted with Gas Chromatography- Mass Spectroscopy. Baghdad Sci.J [Internet]. 2022 Aug. 1 [cited 2022 Nov. 29];19(4):0816. Available from: https://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/5571
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