Sensitive Determination of Hydrochlorothiazide Drug in the Various Samples Via Developed Method of CFIA System
DOI:
https://doi.org/10.21123/bsj.2024.8460Keywords:
Biological samples, CFIA System, Hydrochlorothiazide, O-phenylenediamine, Pharmaceutical formulationAbstract
Hydrochlorothiazide drug determination in pharmaceutical and biological urine samples using a novel continuous flow-injection analysis technique that is rapid, simple, economical, and sensitive. The complex formed by the reaction of hydrochlorothiazide and O-phenylenediamine with potassium ferricyanide to produce an orange-colored product at 480 nm was the basis for the proposed method. Other chemical and physical parameters that affect the stability and development of the colored product used in this developed method includes sample volume, flow rate, reagent concentrations, and reaction coil. The proposed method’s linearity ranges from 5 to 150 μg.mL-1 and its correlation coefficients were 0.9988, and the recovery percentage and error percentage were 100.88 and 0.88, respectively. The detection limit and Limit of quantification values were 2.622 and 7.97. A sample throughput of 90 samples. hour1- . The new approach was effectively employed to determine the presence of hydrochlorothiazide in the pure, biological, and pharmaceutical samples.
Received 25/01/2023
Revised 24/07/2023
Accepted 26/07/2023
Published Online First 20/02/2024
References
Shaikh JS, Raut S, Abdul A, Pathan MA. High-performance liquid chromatographic assay of amlodipine, valsartan, and hydrochlorothiazide simultaneously and its application to pharmaceuticals, urine, and plasma analysis. J Chromatogr B. 2020; 1155: 122295. https://doi.org/10.1016/j.jchromb.2020.122295
Rezk MR, Fayed AS, Marzouk HM, Abbas SS. A validated high-performance thin-layer chromatographic method for the simultaneous determination of Zofenopril calcium and hydrochlorothiazide in the presence of the hydrochlorothiazide impurities: Chlorothiazide and salami. J AOAC Int, 101(4): 1031-1041. https://doi.org/10.5740/jaoacint.17-0095
Abdullah AI, Abass SM. Azo Coupling Reaction for Indirect Spectrophotometric Determination of Furosemide using Resorcinol as a Reagent. In IOP Conference Series: Wood Mater Sci Eng. 2021;1058(1): 012077. https://doi.org/10.1088/1757899X/1058/1/012077
Hapse SA, Wagh VS, Kadaskar PT, Dokhe MD, Shirsath AS. Spectrophotometric estimation and validation of hydrochlorothiazide in tablet dosage forms by using different solvents. Der Pharma Chemica. 2012; 4(1): 10-14. https://dx.doi.org/10.21608/aps.2020.45025.1042
Abdelwahab NS. Spectrophotometric methods for simultaneous determination of Carvedilol and Hydrochlorothiazide in the combined dosage form. Arabian J Chem. 2016; 9: S355-60. https://doi.org/10.1016/j.arabjc.2011.05.002
Alghamdi AF. Electrochemical oxidation behavior of hydrochlorothiazide on a glassy carbon electrode and its voltametric determination in pharmaceutical formulations and biological fluids. J Food Drug Anal .2014; 22(3): 363-9. https://doi.org/10.1016/j.jfda.2013.12.003
Beitollahi H, Hamzavi M, Torkzadeh-Mahani M. Electrochemical determination of hydrochlorothiazide and folic acid in real samples using a modified graphene oxide sheet paste electrode. Mater Sci Eng C Mater Biol Appl .2015; 52: 297-305. https://doi.org/10.1016/j.msec.2015.03.031
Hamed LL, Qassim BB. .Direct and new flow injection method for assay of Iron as ferrous sulfate in pure and dosage forms through the complexation with 2,2 ︡ dipyridyl reagent. Int J Pharm Res. 2020; 12(2): 1329-38. https://doi.org/10.31838/ijpr/2020.SP2.128
Abdullah HJ, Qassim BB. Development and Validation CFIA/MZ System as a Green Method for Determination of Thiol Drug (D-PEN). Egypt J Chem. 2022; 65(1): 1-2. https://doi.org/10.21608/ejchem.2021.80167.3964
Ghafarloo A, Sabzi RE, Samadi N, Hamishehkar H. Spectrofluorimetric Determination of Hydrochlorothiazide by a Carbon Dots-Based Probe via Inner Filtering Effect and Resonance Rayleigh Scattering. J Braz Chem Soc. 2022; 33: 361-8. https://dx.doi.org/10.21577/0103-5053.20210155
Saleem BA. Spectrophotometric determination of some drugs using oxidation-reduction reactions Ibn al-Haitham J Pure Appl. Sci. 2019; 32(3): 43-55. https://doi.org/10.30526/32.3.2281
Al-rashidy AA, Shareef AK. Spectrophotometric Determination of Chlorpromazine Hydrochloride Using 4-Nitroanilline by Oxidative Coupling Reaction. Baghdad Sci J .2019; 16(1): 0194. DOI: https://doi.org/10.21123/bsj.2019.16.1(Suppl.).0194
Fahad AS, Thani MZ, Abdullah AM, Dhahir SA. Development of an Ecological-friendly Method for Ciprofloxacin Determination and Cloud Point Extraction in Pharmaceuticals using Fe (II) (FeSO4. 7H2O). In IOP Conf Ser Mater Sci Eng. 2020; 871: 1-9. https://doi.org/10.1088/1757-899X/871/1/012028
Kadhim EA, Dhahir SA, Sando MS. New Diaz Coupling Reaction, Cloud Point Extraction Spectrophotometric Determination of Sulphadimidine Soudium in Pure form and Pharmacetical Preparation with Salicylic Acid as the Coupling Reaction. Indian J Forensic Med Toxicol .2020; 14(2): 862-868. https://doi.org/10.37506/ijfmt.v14i2.2989
Kadhim MM, AlMashhadani HA, Hashim RD, Khadom AA, Salih KA, et al. Effect of Sr/Mg co-substitution on corrosion resistance properties of hydroxyapatite-coated on Ti– 6Al–4V dental alloys. J Phys Chem Solids. 2022; 161(3): 10450. https://doi.org/10.1016/j.jpcs.2021.110450
Amir R, Hadi H. Spectrophotometric determination of vitamin B1 in dosage forms using drugs compounds as reagents by normal and reverse flow injection methods. Curr Pharm Anal .2022; 18(2): 218-27. http://dx.doi.org/10.2174/1573412917666210118120836
Turkey NS, Jeber JN. Flow Injection Analysis with Turbidity Detection for the Quantitative Determination of Mebeverine Hydrochloride in Pharmaceutical Formulations. Baghdad SciJ .2022; 19(1): 0141. DOI: https://doi.org/10.21123/bsj.2022.19.1.0141
Turkey NS, Mezaal EN. Assessment of long-distance chasing photometer (NAG-ADF-300-2) by estimating the drug atenolol with ammonium molybdate via continuous flow injection analysis. Ibn Al-Haitham J Pure Appl Sci 2020; 17 (1): 78-92. https://doi.org/10.30526/33.1.2383
Khammas ZA, Ahmad SS. Micelle-mediating extraction combined with visible spectrophotometry for the determination of ultra-trace amounts of bendiocarb insecticide in various matrices after oxidative coupling with O-Toluidine. Int Res J Pure Appl Chem. 2016; 10(2): 1-6. https://doi.org/10.9734/IRJPAC/2016/21948
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