Synthesis and Characterization of Some New Benzodiazepinium Salt Derivatives under microwave Irradiation

محتوى المقالة الرئيسي

Abdel- Amir M. Fenjan
Ala'a Sh. Shubram

الملخص

An attempt to synthesize the benzoimidazol derivatives from the reaction of o-phenylenediamine and benzoic acid derivatives in the presence of ethanol and various ketones under microwave irradiation, 1 , 5 - benzodiazepinum salt derivatives were obtained instead of them. Unexpected reaction was happened for synthesis a new series of benzodiazepinium salt derivatives in a selective yield . The reaction mechanism was also discussed. The new compounds were purified and identified their structures were elucidated using various physical techniques like; FT- IR spectra, micro elemental analysis (C.H.N) and 1H NMR spectra.

تفاصيل المقالة

كيفية الاقتباس
1.
Synthesis and Characterization of Some New Benzodiazepinium Salt Derivatives under microwave Irradiation. Baghdad Sci.J [انترنت]. 6 ديسمبر، 2015 [وثق 23 يوليو، 2024];12(4):753-60. موجود في: https://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/2123
القسم
article

كيفية الاقتباس

1.
Synthesis and Characterization of Some New Benzodiazepinium Salt Derivatives under microwave Irradiation. Baghdad Sci.J [انترنت]. 6 ديسمبر، 2015 [وثق 23 يوليو، 2024];12(4):753-60. موجود في: https://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/2123

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