الاستفادة من رنين البلازمون السطحي الموضعي لجسيمات الفضة النانوية لتقدير الطيف الضوئي للأملوديبين وهيدروكلوروثيازيد
DOI:
https://doi.org/10.21123/bsj.2024.8097الكلمات المفتاحية:
أملوديبين، هيدروكلوروثيازيد، جسيمات الفضة النانوية، رنين سطح البلازمون، قياس الطيف الضوئي.الملخص
أملوديبين هو مانع قوي وطويل المفعول لقنوات الكالسيوم. يمكن للمرضى الذين يعانون من ارتفاع ضغط الدم تناوله لعلاج ارتفاع ضغط الدم والذبحة الصدرية وتقليل مخاطر الإصابة بالسكتة الدماغية. يستخدم مدر للبول يسمى هيدروكلوروثيازيد لعلاج الوذمة وارتفاع ضغط الدم. بالإضافة إلى ذلك ، يتم استخدامه لعلاج بعض أنواع مرض السكري وارتفاع السكر في الدم ونقص بوتاسيوم الدم. تتوفر هذه الأدوية على نطاق واسع في السوق وغالبًا ما يتم تناولها عن طريق الفم. وبالتالي ، تم إنشاء طريقة سريعة ودقيقة وآمنة بيئيًا وغير مكلفة لقياس أملوديبين وهيدروكلوروثيازيد والتحقق منها. كانت قدرة الدواء على اختزال Ag + 1 إلى Ag0 مباشرة وإنشاء جزيئات الفضة النانوية (Ag NPs )
في وجود كبريتات لوريل الصوديوم كمثبت أساس الطريقة. ظهر صدى كبير للبلازمون السطحي للجسيمات النانوية المركبة عند 418 نانومتر و 410 نانومتر ، والتي تم استخدامها للكشف الطيفي الكمي للأملوديبين وهيدروكلوروثيازيد. مع حدود الكشف عن 0.442 و 0.128 ميكروغرام /مل ، كانت نطاقات التركيز الخطي للأملوديبين وهيدروكلوروثيازيد 0.5 - 28 و 0.8 - 6 ميكروغرام /مل على التوالي. تم استخدام الطريقة المقترحة لتقييم أشكال الجرعات التجارية التي تحتوي على الأدوية المدروسة بنجاح.
Received 07/12/2023
Revised 28/08/2023
Accepted 30/08/2023
Published Online First 20/04/2024
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الحقوق الفكرية (c) 2024 Rasul Jameel Ali , Lazeeza Sattar Omer , Nagham Nadhim Habeeb , Asmaa Ghanim Dawood
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