تحضير وتشخيص وتطبيق متحسس للغاز لمركب جديد من انابيب الكاربون النانوية: الفثالوسيانين:أوكسيد الفلز

محتوى المقالة الرئيسي

Mohanad Mousa Kareem, Dr.
Burak Yahya Kadem, Dr.
Emman J. Mohammad, Dr.
Abbas Jassim Atiyah, Dr.

الملخص

تم تخليق فثالوسيانين الكوبالت الجديد المعوض (CoPc) باستخدام مواد البدء النفثالين -1،4،5 ، ثنائي هيدريد حامض التراكربونيك (NDI) عن طريق العملية الجافة. تم تصنيع الأوكسيدات المعدنية (60٪ Ni3O440٪ -Co3O4) مع الأنابيب النانوية الكاربونية متعددة الحوائط (F-MWCNTs) لإنتاج المتراكب النانوي (F-MWCNTs / MO)  (E2) وخلطها مع CoPc لإنتاج (F-MWCNT) / CoPc / MO) (E3). تم فحص هذه المركبات باستخدام طرق تحليلية وطيفية مختلفة مثل H-NMR1  ، مطياف FTIR ، حيود الأشعة السينية (PXRD)  (2θ o = 10-80) ، مطيافية رامان ، وقياس الطيف المرئي للأشعة فوق البنفسجية. ثم تم فحص نشاط هذه المواد لاستشعار غازات (NH3 ، ميثانول ، أسيتون).كان تركيز المحاليل المستخدمة 0.2 ملغم من المادة المحضرة  لكل1 مل من الامونيا, الميثانول والاسيتون. تم أجراء القياسات بدرجة حرارة 298 كلفن.  كانت الأشكال السطحية للمواد المحضرة غير متجانسة.

تفاصيل المقالة

كيفية الاقتباس
1.
تحضير وتشخيص وتطبيق متحسس للغاز لمركب جديد من انابيب الكاربون النانوية: الفثالوسيانين:أوكسيد الفلز. Baghdad Sci.J [انترنت]. 1 يونيو، 2021 [وثق 19 مايو، 2024];18(2):0384. موجود في: https://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/5073
القسم
article

كيفية الاقتباس

1.
تحضير وتشخيص وتطبيق متحسس للغاز لمركب جديد من انابيب الكاربون النانوية: الفثالوسيانين:أوكسيد الفلز. Baghdad Sci.J [انترنت]. 1 يونيو، 2021 [وثق 19 مايو، 2024];18(2):0384. موجود في: https://bsj.uobaghdad.edu.iq/index.php/BSJ/article/view/5073

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